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Development of a harmonised method for the profiling of amphetamines: I. Synthesis of standards and compilation of analytical data
National Bureau of Investigation, P.O. Box 285, FIN-01301 Vantaa, Finland.
Swedish National Laboratory of Forensic Science, SKL, SE-581 94 Linköping, Sweden.
Swedish National Laboratory of Forensic Science, SKL, SE-581 94 Linköping, Sweden.
Linköpings universitet, Tekniska högskolan. Linköpings universitet, Institutionen för fysik, kemi och biologi, Organisk Analytisk Kemi.
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2005 (engelsk)Inngår i: Forensic Science International, ISSN 0379-0738, E-ISSN 1872-6283, Vol. 149, nr 2-3, s. 219-229Artikkel i tidsskrift (Fagfellevurdert) Published
Abstract [en]

Reference material was synthesised for 21 substances that are frequently present as synthetic impurities, i.e. by-products, in illicitly produced amphetamine. Each of these substances is a typical by-product for at least one of the three approaches most often used to synthesise amphetamine, namely, the Leuckart, the reductive amination of benzyl methyl ketone, and the nitrostyrene routes. A large body of data on the substances was recorded, including the following: mass spectra, ultraviolet spectra, Fourier transform infrared spectra, infrared spectra in gas phase, and 1H NMR and 13C NMR spectra. © 2004 Elsevier Ireland Ltd. All rights reserved.

sted, utgiver, år, opplag, sider
2005. Vol. 149, nr 2-3, s. 219-229
Emneord [en]
Amphetamine, profiling, impurities, synthesis, infrared spectroscopy, gas chromatography- mass spectrometry, H-NMR, C-NMR, UV
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Identifikatorer
URN: urn:nbn:se:liu:diva-30453DOI: 10.1016/j.forsciint.2004.06.020Lokal ID: 16024OAI: oai:DiVA.org:liu-30453DiVA, id: diva2:251275
Tilgjengelig fra: 2009-10-09 Laget: 2009-10-09 Sist oppdatert: 2017-12-13bibliografisk kontrollert

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