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Synthesis of the novel Zr3AlC2 MAX phase
Katholieke University of Leuven, Belgium; CEN SCK, Belgium.
Linköpings universitet, Institutionen för fysik, kemi och biologi, Tunnfilmsfysik. Linköpings universitet, Tekniska fakulteten. Drexel University, PA 19104 USA.
Linköpings universitet, Institutionen för fysik, kemi och biologi, Tunnfilmsfysik. Linköpings universitet, Tekniska fakulteten.
University of Poitiers, France.
Vise andre og tillknytning
2016 (engelsk)Inngår i: Journal of the European Ceramic Society, ISSN 0955-2219, E-ISSN 1873-619X, Vol. 36, nr 3, s. 943-947Artikkel i tidsskrift (Fagfellevurdert) Published
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Abstract [en]

Herein we report, for the first time, on the synthesis and structural characterization of the Zr-based MAX phase, Zr3AlC2, fabricated by reactive hot pressing of ZrH2, Al, and C powders. The crystal structure of Zr3AlC2 was determined by X-ray diffraction and high resolution transmission electron microscopy to be the hexagonal space group P63/mmc. The a and c lattice parameters are 3.33308(6)angstrom and 19.9507(3)angstrom, respectively. The samples include the secondary phases ZrC and Zr-Al intermetallics as confirmed by quantitative electron probe microanalysis. The Vickers hardness, using a force of 30 N, was measured to be 4.4 +/- 0.4 GPa. (C) 2015 Elsevier Ltd. All rights reserved.

sted, utgiver, år, opplag, sider
ELSEVIER SCI LTD , 2016. Vol. 36, nr 3, s. 943-947
Emneord [en]
MAX phase; X-ray diffraction; Reactive hot pressing; Hydrides
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Identifikatorer
URN: urn:nbn:se:liu:diva-124461DOI: 10.1016/j.jeurceramsoc.2015.10.011ISI: 000367407900066OAI: oai:DiVA.org:liu-124461DiVA, id: diva2:899831
Merknad

Funding Agencies|Agency for Innovation by Science and Technology (IWT), Flanders, Belgium [131081]; European Atomic Energy Communitys (Euratom) Seventh Framework Programme [604862]; Hercules Foundation [ZW09-09]; Swedish Government; Swedish Government Strategic Research Area Grant in Materials Science (MAT-LiU)

Tilgjengelig fra: 2016-02-02 Laget: 2016-02-01 Sist oppdatert: 2017-11-30

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