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Resolving the debated atomic structure of the metastable cubic SiNx tissue phase in nanocomposites with TiN
Linköping University, Department of Physics, Chemistry and Biology, Thin Film Physics. Linköping University, Department of Science and Technology. Linköping University, Faculty of Science & Engineering.
Linköping University, National Supercomputer Centre (NSC). Linköping University, Faculty of Science & Engineering.
Linköping University, Department of Physics, Chemistry and Biology, Theoretical Physics. Linköping University, Faculty of Science & Engineering. Max Planck Inst Eisenforsch GmbH, Germany.
Linköping University, Department of Physics, Chemistry and Biology, Thin Film Physics. Linköping University, Faculty of Science & Engineering.ORCID iD: 0000-0003-3203-7935
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2018 (English)In: Physical Review Materials, ISSN 2475-9953, Vol. 2, no 9, article id 093608Article in journal (Refereed) Published
Abstract [en]

The TiN/SiNx nanocomposite and nanolaminate systems are the archetype for super if not ultrahard materials. Yet, the nature of the SiNx tissue phase is debated. Here, we show by atomically resolved electron microscopy methods that SiNx is epitaxially stabilized in a NaCl structure on the adjacent TiN(001) surfaces. Additionally, electron energy loss spectroscopy, supported by first-principles density functional theory calculations infer that SiNx hosts Si vacancies.

Place, publisher, year, edition, pages
American Physical Society, 2018. Vol. 2, no 9, article id 093608
National Category
Condensed Matter Physics
Identifiers
URN: urn:nbn:se:liu:diva-151780DOI: 10.1103/PhysRevMaterials.2.093608ISI: 000445181600001OAI: oai:DiVA.org:liu-151780DiVA, id: diva2:1254061
Note

Funding Agencies|Swedish Research Council (VR) [2008-405, 2012-4359, 2015-04391, 2016-04412]; Swedish Foundation for Strategic Research (SSF) through FunCase; SRL [10-0026]; M. Bergwall foundation; Swedish Government Strategic Research Area in Materials Science on Functional Materials at Linkoping University [2009 00971]; Ministry of Education and Science of the Russian Federation [14.Y26.31.0005, K2-2017-080]; [RIF 14-0074]

Available from: 2018-10-08 Created: 2018-10-08 Last updated: 2018-11-14Bibliographically approved

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Olovsson, Weine

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