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INFLUENCE OF THE SEPARATION PARAMETERS APPLIED FOR DETERMINATION OF IMPURITIES FDG AND CLDG
University of Politehn Bucuresti, Romania; Horia Hulubei National Institute Phys and Nucl Engn, Romania.
Horia Hulubei National Institute Phys and Nucl Engn, Romania.
University of Politehn Bucuresti, Romania.
Linköping University, Department of Medical and Health Sciences. Linköping University, Faculty of Medicine and Health Sciences. Region Östergötland, Center for Surgery, Orthopaedics and Cancer Treatment, Department of Radiation Physics.
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2017 (English)In: Farmacia, ISSN 0014-8237, E-ISSN 2065-0019, Vol. 65, no 1, 153-158 p.Article in journal (Refereed) Published
Abstract [en]

2-fluoro-2-deoxy-D-glucose (FDG) and 2-chloro-2-deoxy-D-glucose (CIDG) are chemical impurities found in the 2-[F-18]fluoro-2-deoxy-D-glucose products (F-18-FDG). The objective of this study was to find the best condition for the separation of FDG and CIDG, evaluating different columns under various operating conditions. Chromatographic parameters such as column temperature, composition and flow rate of the mobile phase were the independent variables used in the optimization process. The optimized method was validated and validation results showed a good accuracy, repeatability and reproducibility.

Place, publisher, year, edition, pages
SOC STINTE FARMACEUTICE ROMANIA , 2017. Vol. 65, no 1, 153-158 p.
Keyword [en]
Chemical impurities; radio-HPAEC; validation
National Category
Chemical Process Engineering
Identifiers
URN: urn:nbn:se:liu:diva-136189ISI: 000394478400024OAI: oai:DiVA.org:liu-136189DiVA: diva2:1086618
Note

Funding Agencies|Sectorial Operational Programme Human Resources Development (SOP HRD) from the European Social Fund; Romanian Government [POSDRU/159/1.5/S/137390/]

Available from: 2017-04-03 Created: 2017-04-03 Last updated: 2017-04-03

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