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Obtaining Silicon Oxide Nanoparticles Doped with Fluorine and Gold Particles by the Pulsed Plasma-Chemical Method
Tomsk Polytech Univ, Russia.
Tomsk Polytech Univ, Russia.
Tomsk Polytech Univ, Russia.
Linköping University, Department of Physics, Chemistry and Biology, Thin Film Physics. Linköping University, Faculty of Science & Engineering.
2019 (English)In: Journal of Nanotechnology, ISSN 1687-9503, E-ISSN 1687-9511, article id 7062687Article in journal (Refereed) Published
Abstract [en]

This paper presents a study on pulsed plasma-chemical synthesis of fluorine- and gold-doped silicon oxide nanopowder. The gold- and fluorine-containing precursors were gold chloride (AuCl3) and sulphur hexafluoride (SF6). Pulsed plasma-chemical synthesis is realized on the laboratory stand, including a plasma-chemical reactor and TEA-500 electron accelerator. The parameters of the electron beam are as follows: 400-450keV electron energy, 60ns half-amplitude pulse duration, up to 200J pulse energy, and 5cm beam diameter. We confirmed the composite structure of SixOy@Au by using transmission electron microscopy and energy-dispersive spectroscopy. We determined the chemical composition and morphology of synthesized SixOy@Au and SixOy@F nanocomposites. The material contained a SixOy@Au carrier with an average size of 50-150nm and a shell of fine particles with an average size of 5-10nm.

Place, publisher, year, edition, pages
HINDAWI LTD , 2019. article id 7062687
National Category
Inorganic Chemistry
Identifiers
URN: urn:nbn:se:liu:diva-164514DOI: 10.1155/2019/7062687ISI: 000461679700001OAI: oai:DiVA.org:liu-164514DiVA, id: diva2:1416449
Note

Funding Agencies|Russian Science FoundationRussian Science Foundation (RSF) [17-73-10269]

Available from: 2020-03-23 Created: 2020-03-23 Last updated: 2020-03-23

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Zhirkov, Igor

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