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Study of Dislocations in Homoepitaxially and Heteroepitaxially Grown AlN Layers
Tokyo Univ Agr & Technol, Japan.
Tokyo Univ Agr & Technol, Japan.
Tokuyama Corp, Japan.
Tokuyama Corp, Japan.
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2020 (English)In: Physica Status Solidi (a) applications and materials science, ISSN 1862-6300, E-ISSN 1862-6319, Vol. 217, no 24, article id 2000465Article in journal (Refereed) Published
Abstract [en]

Dislocation densities in AlN layers grown on c-plane sapphire and physical vapor transport-grown AlN (PVT-AlN) (0001) substrates, by metalorganic vapor phase epitaxy (MOVPE) and hydride vapor phase epitaxy (HVPE), respectively, are evaluated from the density of etch pits formed in sodium hydroxide (NaOH)/potassium hydroxide (KOH) eutectic heated to 450 degrees C. In the heteroepitaxial layers grown by MOVPE on the sapphire substrates, etch pits with different sizes are formed. Cross-sectional transmission electron microscopy (TEM) observations reveal that the large, medium, and small pits, with densities of 1.4 x 10(6), 2.6 x 10(7), and 6.9 x 10(9) cm(-2), respectively, correspond to screw, mixed, and edge dislocations, respectively. In contrast, in the homoepitaxial layers grown by HVPE on the PVT-AlN substrates, only one kind of etch pit with uniform size corresponding to the edge dislocations is formed with a density of 10(3)-10(4) cm(-2). Cross-sectional TEM observation confirms that the edge dislocations in the homoepitaxial layer propagate from the substrate through the interface, which indicates that the dislocation density does not increase during homoepitaxial growth by HVPE. The HVPE-AlN homoepitaxial layers grown on the PVT-AlN substrates are found to have very low dislocation density.

Place, publisher, year, edition, pages
WILEY-V C H VERLAG GMBH , 2020. Vol. 217, no 24, article id 2000465
Keywords [en]
aluminum nitride; dislocations; etch pits; hydride vapor phase epitaxy; ultrawide bandgap semiconductor
National Category
Condensed Matter Physics
Identifiers
URN: urn:nbn:se:liu:diva-171396DOI: 10.1002/pssa.202000465ISI: 000583248700001OAI: oai:DiVA.org:liu-171396DiVA, id: diva2:1504677
Note

Funding Agencies|Institute of Global Innovation Research, Tokyo University of Agriculture and Technology, Japan

Available from: 2020-11-30 Created: 2020-11-30 Last updated: 2022-10-26

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