Development of a harmonised method for the profiling of amphetamines: I. Synthesis of standards and compilation of analytical data
2005 (English)In: Forensic Science International, ISSN 0379-0738, E-ISSN 1872-6283, Vol. 149, no 2-3, 219-229 p.Article in journal (Refereed) Published
Reference material was synthesised for 21 substances that are frequently present as synthetic impurities, i.e. by-products, in illicitly produced amphetamine. Each of these substances is a typical by-product for at least one of the three approaches most often used to synthesise amphetamine, namely, the Leuckart, the reductive amination of benzyl methyl ketone, and the nitrostyrene routes. A large body of data on the substances was recorded, including the following: mass spectra, ultraviolet spectra, Fourier transform infrared spectra, infrared spectra in gas phase, and 1H NMR and 13C NMR spectra. © 2004 Elsevier Ireland Ltd. All rights reserved.
Place, publisher, year, edition, pages
2005. Vol. 149, no 2-3, 219-229 p.
Amphetamine, profiling, impurities, synthesis, infrared spectroscopy, gas chromatography- mass spectrometry, H-NMR, C-NMR, UV
IdentifiersURN: urn:nbn:se:liu:diva-30453DOI: 10.1016/j.forsciint.2004.06.020Local ID: 16024OAI: oai:DiVA.org:liu-30453DiVA: diva2:251275