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Synthesis, characterization and optical power limiting behaviour of phenylazo- and 4-nitrophenylazo-tetrahydroxytetrathiacalix[4]arene
Univ Lyon 1, CNRS, UMR 5615, Lab Multimat & Interfaces, F-69622 Villeurbanne, France Swedish Def Res Agcy FOI, Div Sensor Technol, SE-58111 Linkoping, Sweden Univ Lyon 1, CNRS, UMR 5078, Lab Synth & Reconnaissance & Org Mol & Biomol, F-69622 Villeurbanne, France.
Univ Lyon 1, CNRS, UMR 5615, Lab Multimat & Interfaces, F-69622 Villeurbanne, France Swedish Def Res Agcy FOI, Div Sensor Technol, SE-58111 Linkoping, Sweden Univ Lyon 1, CNRS, UMR 5078, Lab Synth & Reconnaissance & Org Mol & Biomol, F-69622 Villeurbanne, France.
Univ Lyon 1, CNRS, UMR 5615, Lab Multimat & Interfaces, F-69622 Villeurbanne, France Swedish Def Res Agcy FOI, Div Sensor Technol, SE-58111 Linkoping, Sweden Univ Lyon 1, CNRS, UMR 5078, Lab Synth & Reconnaissance & Org Mol & Biomol, F-69622 Villeurbanne, France.
Univ Lyon 1, CNRS, UMR 5615, Lab Multimat & Interfaces, F-69622 Villeurbanne, France Swedish Def Res Agcy FOI, Div Sensor Technol, SE-58111 Linkoping, Sweden Univ Lyon 1, CNRS, UMR 5078, Lab Synth & Reconnaissance & Org Mol & Biomol, F-69622 Villeurbanne, France.
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2001 (English)In: Journal of Materials Chemistry, ISSN 0959-9428, E-ISSN 1364-5501, Vol. 11, no 12, 3014-3017 p.Article in journal (Refereed) Published
Abstract [en]

p-Tetrakis(4-nitrophenylazo) tetrahydroxytetrathiacalix[4] arene and p-tetrakis(phenylazo) tetrahydroxytetrathiacalix[4] arene were prepared and fully characterized using H-1 and C-13 NMR, mass spectroscopy, thermogravimetric analysis and differential scanning calorimetry. The solid-state structure of p-tetrakis(4-nitrophenylazo) tetrahydroxytetrathiacalix[4] arene was investigated by single crystal X-ray diffraction. It crystallized in the triclinic system (space group: P (1) over bar). z-Scan experiments were performed on the p-tetrakis(4-nitrophenylazo) tetrahydroxytetrathiacalix[ 4] arene showing non linear absorption due to two photon absorption with a TPA cross-section of about 50 x 10(-50) cm(4) s per photon. Optical power limiting measurements on the p-tetrakis( phenylazo) tetrahydroxytetrathiacalix[ 4] arene at 532 nm (48% linear transmission) was found to limit the energy to similar to9 muJ.

Place, publisher, year, edition, pages
2001. Vol. 11, no 12, 3014-3017 p.
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Natural Sciences
Identifiers
URN: urn:nbn:se:liu:diva-49047OAI: oai:DiVA.org:liu-49047DiVA: diva2:269943
Available from: 2009-10-11 Created: 2009-10-11 Last updated: 2017-12-12

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