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A Novel Oxide Characterization Method of Nickel Base Alloy 600 Used in Nuclear Plant Reactors
Linköping University, Department of Physics, Chemistry and Biology, Thin Film Physics. Linköping University, The Institute of Technology. (Tunnfilmsfysik, Thin Film Physics)ORCID iD: 0000-0003-3277-1945
Studsvik Nuclear AB.
The Japan Atomic Power Company.
Linköping University, Department of Physics, Chemistry and Biology, Thin Film Physics. Linköping University, The Institute of Technology. (Tunnfilmsfysik, Thin Film Physics)ORCID iD: 0000-0002-2837-3656
2013 (English)In: / [ed] F. Marquis, Hoboken, NJ, USA: John Wiley & Sons, 2013, 415- p.Conference paper, Published paper (Refereed)
Abstract [en]

The Alloy 600 is a polycrystalline nickel base alloy used in pressurized water reactors (PWR) of nuclear power plants. Long term exposure of the alloy to primary water of PWR generates an oxide film that strongly influences the stress corrosion cracking behavior of the alloy. Recently, it has been shown that the oxide film structure, composition and thickness depend on the dissolved hydrogen content in the primary water. In this work we have explored a novel approach which enables a high spatial resolution oxide thickness measurement by nanomechanical testing. Oxide films have been grown on Alloy 600 specimens exposed between 5000 and 35000 hours at 320-330°C with hydrogen levels in the range 5 to 25 mL H2/kg H2O. A Triboindenter TI-950 from Hysitron was used to measure the change of nanomechanical properties in polished cross-sections. The increase of hardness has been correlated to the presence of oxides.

Place, publisher, year, edition, pages
Hoboken, NJ, USA: John Wiley & Sons, 2013. 415- p.
National Category
Engineering and Technology
Identifiers
URN: urn:nbn:se:liu:diva-102574DOI: 10.1002/9781118792148.ch415OAI: oai:DiVA.org:liu-102574DiVA: diva2:679327
Conference
PRICM: 8 Pacific Rim International Congress on Advanced Materials and Processing
Note

E. Broitman and L. Hultman acknowledge the Swedish Government Strategic Research Area in Materials Science on Functional Materials at Linköping University (Faculty Grant SFO-Mat-LiU # 2009-00971).

Available from: 2013-12-14 Created: 2013-12-14 Last updated: 2016-08-31Bibliographically approved

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Broitman, EstebanHultman, Lars

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