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Stability of (B4C)-B-10 thin films under neutron radiation
Linköping University, Department of Physics, Chemistry and Biology. European Spallat Source ESS AB, Sweden.
Technical University of Munich, Germany.
Technical University of Munich, Germany.
Linköping University, Department of Physics, Chemistry and Biology, Thin Film Physics. Linköping University, Faculty of Science & Engineering.
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2015 (English)In: Radiation Physics and Chemistry, ISSN 0969-806X, E-ISSN 1879-0895, Vol. 113, 14-19 p.Article in journal (Refereed) Published
Abstract [en]

Thin films of (B4C)-B-10 have shown to be very suitable as neutron-converting material in the next generation of neutron detectors, replacing the previous predominantly used He-3. In this contribution we show under realistic conditions that (B4C)-B-10 films are not damaged by the neutron irradiation and interactions, which they will be exposed to under many years in a neutron detector. 1 mu m thick (B4C)-B-10 thin films were deposited onto Al or Si substrates using dc magnetron sputtering. As-deposited films were exposed to a cold neutron beam with fluences of up to 1.1 x 10(14) cm(-2) and a mean wavelength of 6.9 angstrom. Both irradiated and as-deposited reference samples were characterized with time-of-flight elastic recoil detection analysis, scanning electron microscopy, transmission electron microscopy, X-ray photoemission spectroscopy, and X-ray diffraction. We show that only 1.8 ppm of the B-10 atoms were consumed and that the film composition does not change by the neutron interaction within the measurement accuracy. The irradiation does not deteriorate the film adhesion and there is no indication that it results in increased residual stress values of the as-deposited films of 0.095 GPa. From what is visible with the naked eye and down to atomic level studies, no change from the irradiation could be found using the above-mentioned characterization techniques.

Place, publisher, year, edition, pages
Elsevier , 2015. Vol. 113, 14-19 p.
Keyword [en]
Neutron; Radiation damage; Thin film; (B4C)-B-10; Neutron detection
National Category
Inorganic Chemistry
Identifiers
URN: urn:nbn:se:liu:diva-120133DOI: 10.1016/j.radphyschem.2015.04.006ISI: 000356196600003OAI: oai:DiVA.org:liu-120133DiVA: diva2:841659
Note

Funding Agencies|Knut and Alice Wallenberg Foundation; Isotope Project; Swedish Government Strategic Research Area in Materials Science on Advanced Functional Materials (AFM) at Linkoping University (SFO-Mat-LiU) [2009-2500971]; Linkoping University

Available from: 2015-07-14 Created: 2015-07-13 Last updated: 2016-08-31

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Höglund, CarinaJensen, JensGreczynski, GrzegorzLu, JunHultman, LarsBirch, Jens
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Department of Physics, Chemistry and BiologyThin Film PhysicsFaculty of Science & Engineering
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Radiation Physics and Chemistry
Inorganic Chemistry

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