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Synthesis of the new MAX phase Zr2AlC
Katholieke University of Leuven, Belgium; CEN SCK, Belgium.
CEN SCK, Belgium.
University of Poitiers, France.
Linköping University, Department of Physics, Chemistry and Biology, Thin Film Physics. Linköping University, Faculty of Science & Engineering. Drexel University, PA 19104 USA.
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2016 (English)In: Journal of the European Ceramic Society, ISSN 0955-2219, E-ISSN 1873-619X, Vol. 36, no 8, 1847-1853 p.Article in journal (Refereed) PublishedText
Abstract [en]

This study reports on the first experimental evidence of the existence of the Zr2AlC MAX phase, synthesised by means of reactive hot pressing of a ZrH2, Al and C powder mixture. The crystal structure of this compound was investigated by X-ray and neutron diffraction. The lattice parameters were determined and confirmed by high-resolution transmission electron microscopy. The effect of varying the synthesis temperature was investigated, indicating a relatively narrow temperature window for the synthesis of Zr2AlC. ZrC was always present as a secondary phase by hot pressing in the 1475-1575 degrees C range.

Place, publisher, year, edition, pages
ELSEVIER SCI LTD , 2016. Vol. 36, no 8, 1847-1853 p.
Keyword [en]
MAX phase ceramics; Diffraction analysis; Reactive hot pressing
National Category
Inorganic Chemistry
Identifiers
URN: urn:nbn:se:liu:diva-127738DOI: 10.1016/j.jeurceramsoc.2016.02.044ISI: 000374082900001OAI: oai:DiVA.org:liu-127738DiVA: diva2:927537
Note

Funding Agencies|Agency for Innovation by Science and Technology (IWT), Flanders, Belgium [131081]; European Atomic Energy Communitys (Euratom) Seventh Framework Programme FP7 [604862]; EERA (European Energy Research Alliance) Joint Programme on Nuclear Materials (JPNM); Hercules Foundation [ZW09-09]; Swedish Foundation for Strategic Research through the Synergy Grant FUNCASE; Swedish Foundation for Strategic Research through the Future Research Leaders 5 program

Available from: 2016-05-12 Created: 2016-05-12 Last updated: 2016-08-31

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Available from 2017-03-02 00:00

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Halim, JosephLu, JunHultman, LarsEklund, PerRosén, JohannaBarsoum, Michel
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