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  • 1.
    Mihon, Mirela
    et al.
    University of Politehn Bucuresti, Romania; Horia Hulubei National Institute Phys and Nucl Engn, Romania.
    Stelian Tuta, Catalin
    Horia Hulubei National Institute Phys and Nucl Engn, Romania.
    Catrinel Ion, Alina
    University of Politehn Bucuresti, Romania.
    Koziorowski, Jacek
    Linköping University, Department of Medical and Health Sciences. Linköping University, Faculty of Medicine and Health Sciences. Region Östergötland, Center for Surgery, Orthopaedics and Cancer Treatment, Department of Radiation Physics.
    Niculae, Dana
    Horia Hulubei National Institute Phys and Nucl Engn, Romania.
    Lavric, Vasile
    University of Politehn Bucuresti, Romania.
    Draganescu, Doina
    Horia Hulubei National Institute Phys and Nucl Engn, Romania; Carol Davila University of Medical and Pharm, Romania.
    INFLUENCE OF THE SEPARATION PARAMETERS APPLIED FOR DETERMINATION OF IMPURITIES FDG AND CLDG2017In: Farmacia, ISSN 0014-8237, E-ISSN 2065-0019, Vol. 65, no 1, p. 153-158Article in journal (Refereed)
    Abstract [en]

    2-fluoro-2-deoxy-D-glucose (FDG) and 2-chloro-2-deoxy-D-glucose (CIDG) are chemical impurities found in the 2-[F-18]fluoro-2-deoxy-D-glucose products (F-18-FDG). The objective of this study was to find the best condition for the separation of FDG and CIDG, evaluating different columns under various operating conditions. Chromatographic parameters such as column temperature, composition and flow rate of the mobile phase were the independent variables used in the optimization process. The optimized method was validated and validation results showed a good accuracy, repeatability and reproducibility.

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