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Non-equilibrium solidification complexions in additive manufacturing enable exceptional creep resistance: An example in nickel-based superalloys
Xi An Jiao Tong Univ, Peoples R China.
Xi An Jiao Tong Univ, Peoples R China.
Linköping University, Department of Management and Engineering, Engineering Materials. Linköping University, Faculty of Science & Engineering.ORCID iD: 0000-0001-7117-9480
Dalian Univ Technol, Peoples R China.
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2025 (English)In: International journal of plasticity, ISSN 0749-6419, E-ISSN 1879-2154, Vol. 191, article id 104379Article in journal (Refereed) Published
Abstract [en]

Insufficient time-dependent properties at elevated temperatures, particularly creep resistance and ductility, are currently crucial factors impeding the use of additively manufactured Hastelloy X (HX). To address this limitation, a micro-nano olive-shaped carbide network was purposely introduced into HX via laser powder bed fusion (L-PBF) and following optimized heat treatment. The inherent chemical heterogeneity combined with the sufficient stored energy of boundaries, induced by the ultrafast cooling rate of the L-PBF process, creates favorable conditions for the formation of micro-nano precipitate networks. Compared to its untreated counterpart, the optimized HX exhibited considerably improved creep resistance, with an 85 % increase in creep life and a 122 % improvement in fracture ductility. Furthermore, through multiscale characterization techniques and theoretical calculations, the preferential precipitation behavior of the micro-nano carbide networks was systematically investigated from both kinetic and thermodynamic perspectives. The superior creep resistance of the L-PBF HX, decorated with carbide networks, stems from the synergistic effects of the high cavity surface energy, effective pinning for grain boundary sliding, and reduced plasticity-assisted diffusion rate, which markedly inhibit the nucleation and growth of microvoids during high-temperature deformations. This work provides a comprehensive understanding of the strengthening mechanisms associated with non-equilibrium solidification-facilitated carbide networks, providing new insights into the targeted design and optimization of L-PBF alloys.

Place, publisher, year, edition, pages
PERGAMON-ELSEVIER SCIENCE LTD , 2025. Vol. 191, article id 104379
Keywords [en]
Additive manufacturing; Nickel-based superalloys; Creep resistance; Fracture ductility; Non-equilibrium solidification
National Category
Applied Mechanics
Identifiers
URN: urn:nbn:se:liu:diva-216477DOI: 10.1016/j.ijplas.2025.104379ISI: 001517265400001Scopus ID: 2-s2.0-105012221548OAI: oai:DiVA.org:liu-216477DiVA, id: diva2:1990207
Note

Funding Agencies|National Natural Science Foundation of China [52201140, 92360307]; Foundation for Young Scholars of Shaanxi Province, China [2023-JC-QN-0521]; National Key Lab of Aerospace Power System and Plasma Technology Foundation [APSPT202301004]; Swedish Governmental Agency for Innovation Systems (Vionnva) [2016-05175]; Centre for Additive Manufacturing-metal (CAM2); AFM at Linkoping University [2009-00971]

Available from: 2025-08-19 Created: 2025-08-19 Last updated: 2025-08-19

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Moverare, Johan

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