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Design for Recycling: Polyester- and Polycarbonate-Based A–B–A Block Copolymers and Their Recyclability Back to Monomers
Wallenberg Wood Science Center, WWSC, Department of Fibre and Polymer Technology, KTH Royal Institute of Technology, Teknikringen 56-58, 100 44 Stockholm, Sweden.
Wallenberg Wood Science Center, WWSC, Department of Fibre and Polymer Technology, KTH Royal Institute of Technology, Teknikringen 56-58, 100 44 Stockholm, Sweden.ORCID iD: 0000-0002-5081-1835
Wallenberg Wood Science Center, WWSC, Department of Fibre and Polymer Technology, KTH Royal Institute of Technology, Teknikringen 56-58, 100 44 Stockholm, Sweden.ORCID iD: 0000-0002-7790-8987
Wallenberg Wood Science Center, WWSC, Department of Fibre and Polymer Technology, KTH Royal Institute of Technology, Teknikringen 56-58, 100 44 Stockholm, Sweden.ORCID iD: 0000-0002-5850-8873
2023 (English)In: Macromolecules, ISSN 0024-9297, E-ISSN 1520-5835, Vol. 56, no 10, p. 3641-3649Article in journal (Refereed) Published
Abstract [en]

Chemical recycling to monomers (CRMs) of A−B−A block copolymers is governed by the chemical structure andthereby the thermodynamic behavior of different block constitu-ents. Here, we show how a thermodynamic toolkit based on acyclic monomer structure and solvent properties can be utilized inthe design of recyclable A−B−A block copolymers with varyingmaterial properties. By combining four cyclic monomers lactide, ε-decalactone, 2,2-diethyltrimethylene carbonate, and trimethylenecarbonate, three different block copolymers were created, suitablefor different CRM scenarios. The chemical structure of the softmidblock (ε-decalactone or trimethylene carbonate) appeared tohave a critical impact both on the ring-closing depolymerizationbehavior and mechanical properties, where changing from apolyester to a polycarbonate soft block increased Young’s modulus from 14 to 200 MPa. Hence, this work demonstrates thecomplexity as well as the opportunities in the design of macromolecular structures for a circular economy.

Place, publisher, year, edition, pages
2023. Vol. 56, no 10, p. 3641-3649
National Category
Polymer Chemistry
Identifiers
URN: urn:nbn:se:liu:diva-207521DOI: 10.1021/acs.macromol.3c00274ISI: 001010158200001Scopus ID: 2-s2.0-85161064993OAI: oai:DiVA.org:liu-207521DiVA, id: diva2:1896638
Funder
Knut and Alice Wallenberg FoundationAvailable from: 2024-09-10 Created: 2024-09-10 Last updated: 2026-01-29

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